二萘并[2,1-b:1',2'-d]呋喃合成路线 （共 25 条）
反应条件
bei der Destillation;
参考文献
Marschalk
Bulletin de la Societe Chimique de France, 1928 , vol. <4> 43, p. 1394
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Corbellini; Aymar
Giorn. Chim. ind. appl., vol. 10, p. 198
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Comp. nat. Mat. color.
Patent: DE469553 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 1392
反应条件
1: binaphtho[2,1-b:1',2'-d]furan With lithium in diethyl ether
T=20°C;
2: chlorodiphenylphosphine oxide in diethyl ether
T=20°C;
参考文献
Luo, Yunfei; Wang, Feng; Zhu, Gangguo; Zhang, Zhaoguo
Tetrahedron Asymmetry, 2004 , vol. 15, # 1 p. 17 - 19
反应条件
1: 68 percent / glac. HOAc / 0.17 h / Heating
2: 300 mg / (1R)-(-)-camphor-10-sulfonyl chloride / pyridine / 0.5 h / 100 °C
View Scheme
参考文献
Kadyrov, Renat; Heinicke, Joachim; Kindermann, Markus K.; Heller, Detlef; Fischer, Christine; Selke, Ruediger; Fischer, Axel K.; Jones, Peter G.
Chemische Berichte, 1997 , vol. 130, # 11 p. 1663 - 1670
反应条件
1: With lithium in diethyl ether; toluene
T=20°C; 3 h;
2: With 1,1,2,2-tetrabromoethane in diethyl ether; toluene
T=-40 - 20°C; 2 h;
参考文献
Ma, Fangfang; Xie, Xiaomin; Zhang, Lei; Peng, Zhiyong; Ding, Lina; Fu, Lei; Zhang, Zhaoguo
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5279 - 5285
参考文献
Clemo; Spence
Journal of the Chemical Society, 1928 , p. 2818
