三甲基-[(E)-2-苯乙烯基]硅烷合成路线 (共 34 条)
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I) in 1,4-dioxane T=90°C; Narasaka acylation; 24 h;
参考文献
Thiot, Carine; Mioskowski, Charles; Wagner, Alain
European Journal of Organic Chemistry, 2009 , # 19 p. 3219 - 3227
反应条件
aluminium trichloride in dichloromethane 1.) -77 deg C, 30 min; 2.) from -77 deg C to r.t.;
参考文献
Brook, Michael A.; Henry, Courtney; Jefferson, Elizabeth; Jueschke, Ralf; Sebastian, Thomas; et al.
Bulletin de la Societe Chimique de France, 1995 , vol. 132, p. 559 - 568
反应条件
2: CsF / dimethylformamide 3: H2 / Pd/C View Scheme
参考文献
Atkinson, Robert S.; Coogan, Michael P.; Lochrie, Ian S. T.
Tetrahedron Letters, 1996 , vol. 37, # 29 p. 5179 - 5182
反应条件
aluminium trichloride in dichloromethane T=0°C; 0.5 h;
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
反应条件
1: Pd(OAc)2 2: 35 percent Chromat. / HBF4 / acetonitrile / 2.07 h / 25 °C View Scheme
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1959 - 1964
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=25°C; 0.2 h; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Ikenaga, Kazutoshi; Wada, Fumio; Matsuda, Tsutomu
Chemistry Letters, 1983 , p. 1337 - 1340
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=40°C; 2 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 25, # 50 p. 5789 - 5792
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=25°C; 0.2 h; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Ikenaga, Kazutoshi; Wada, Fumio; Matsuda, Tsutomu
Chemistry Letters, 1983 , p. 1337 - 1340
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=25°C; Yield given. Yields of byproduct given;
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1959 - 1964
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=25°C; Yield given. Yields of byproduct given;
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1959 - 1964