1-(4-甲氧苯基)-4-苯偶氮基丁啶-2-酮合成路线 (共 19 条)
反应条件
trifluoroacetic acid 6 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2105 - 2111
反应条件
zinc; iodine in 1,4-dioxane
T=25°C; 5 h; ultrasonication;
参考文献
Bose, Ajay K.; Gupta, Kavita; Manhas, M. S.
Journal of the Chemical Society, Chemical Communications, 1984 , # 2 p. 86 - 87
反应条件
diethylzinc; RhCl(PPh3)3 in hexane; toluene
T=40°C; 0.5 h;
参考文献
Kanai, Kazuo; Wakabayashi, Hitoshi; Honda, Toshio
Heterocycles, 2002 , vol. 58, p. 47 - 51
反应条件
zinc; bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran
T=20°C; Reformatsky reaction; 0.1 h;
参考文献
Chen, Lei; Zhao, Gang; Ding, Yu
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2611 - 2614
反应条件
nickel in acetone
3 h; Heating;
参考文献
Kanwar, Seema; Sharma
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 5 p. 1121 - 1128
反应条件
titanium tetrachloride; triethylamine in dichloromethane
T=0°C; 3 h;
参考文献
Annunziata, Rita; Benaglia, Maurizio; Cinquini, Mauro; Cozzi, Franco; Scolaro, Alessandra
Gazzetta Chimica Italiana, 1995 , vol. 125, # 2 p. 65 - 68
反应条件
chloro-trimethyl-silane; zinc in benzene
2.5 h; Heating;
参考文献
Palomo, Claudio; Cossio, Fernando P.; Arrieta, Ana; Odriozola, Jose M.; Oiarbide, Mikel; Ontoria, Jesus M.
Journal of Organic Chemistry, 1989 , vol. 54, # 24 p. 5736 - 5745
反应条件
1: With 1,2-di-iodoethane; zinc in tetrahydrofuran
T=43°C; Reformatsky Reaction; 2 h; Sonication;
2: With hydrogenchloride in water
Reformatsky Reaction;
参考文献
Lee, Adam Shih-Yuan; Chang, Yu-Ting; Su, Feng-Yi
Journal of the Chinese Chemical Society, 2014 , vol. 61, # 2 p. 290 - 294
反应条件
ethylmagnesium bromide in tetrahydrofuran
14 h;
参考文献
Kano, Shinzo; Ebata, Tsutomu; Shibuya, Shiroshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2105 - 2111
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
controlled-potential electrolysis, -1.3 V;
参考文献
Casadei, Maria Antonietta; Inesi, Achille; Moracci, Franco Micheletti; Occhialini, Donatella
Tetrahedron, 1989 , vol. 45, # 21 p. 6885 - 6890