1,1-二乙氧基-3-苯基-2-丙酮合成路线 （共 11 条）
反应条件
in tetrahydrofuran T=-78°C; 2 h;
参考文献
Adamczyk, Maciej; Johnson, Donald D.; Mattingly, Phillip G.; Pan, You; Reddy, Rajarathnam E.
Synthetic Communications, 2002 , vol. 32, # 20 p. 3199 - 3205
反应条件
hydrogenchloride in dichloromethane T=20°C; 12 h;
参考文献
Grecian, Scott; Desai, Pankaj; Mossman, Craig; Poutsma, Jennifer L.; Aube, Jeffrey
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9439 - 9447
反应条件
ammonium chloride in tetrahydrofuran; hexane; ethyl acetate
参考文献
Gambhir, Sanjiv S.; Levi, Jelena; De, Abhijit
Patent: US2009/75309 A1, 2009 ;
反应条件
1: aq. HClO4 / dioxane / 25 °C 2: TsOH View Scheme
参考文献
Dahn,H. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1000 - 1006
反应条件
2: aq. H3PO4 3: TsOH View Scheme
参考文献
Dahn,H. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1000 - 1006
反应条件
toluene-4-sulfonic acid
参考文献
Dahn,H. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1000 - 1006
反应条件
hydrogenchloride in ethanol; water Reflux;
参考文献
UNIVERSITA DEGLI STUDI DI SIENA; GIULIANI, Germano; CAPPELLI, Andrea; VOMERO, Salvatore; ANZINI, Maurizio
Patent: WO2011/7314 A1, 2011 ;
Location in patent: Page/Page column 38 ;
反应条件
1.1: C24H34N2O2; N-(2-hydroxybenzyl)amine / toluene / 72 h / |Reflux 1.2: 20 °C 2.1: triethylamine / dichloromethane 3.1: hydrogenchloride / tetrahydrofuran; water / 0 °C 5.1: hydrogenchloride / water; 1,4-dioxane / 100 °C View Scheme
参考文献
Pan, Hongjie; Xie, Ying; Liu, Mao; Shi, Yian
RSC Advances, 2014 , vol. 4, # 5 p. 2389 - 2392
反应条件
1.1: C24H34N2O2; N-(2-hydroxybenzyl)amine / toluene / 72 h / |Reflux 1.2: 20 °C 2.1: triethylamine / dichloromethane 3.1: hydrogenchloride / tetrahydrofuran; water / 0 °C View Scheme
参考文献
Pan, Hongjie; Xie, Ying; Liu, Mao; Shi, Yian
RSC Advances, 2014 , vol. 4, # 5 p. 2389 - 2392
反应条件
hydrogenchloride in ethanol
Heating;
参考文献
Levi, Jelena; De, Abhijit; Cheng, Zhen; Gambhir, Sanjiv Sam
Journal of the American Chemical Society, 2007 , vol. 129, # 39 p. 11900 - 11901
