(E)-4-溴-N’-羟基苄脒合成路线 （共 27 条）
反应条件
Me3SiN=S=NSiMe3 in benzene T=5 - 10°C; 1.5 h;
参考文献
Russian Chemical Bulletin, , vol. 42, # 4 p. 706 - 708
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 742 - 743
反应条件
1: 29 percent / benzene / 1.5 h / 5 - 10 °C 2: 98 percent / benzene / 48 h / 20 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 42, # 4 p. 706 - 708
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 742 - 743
反应条件
in benzene T=5 - 10°C; 1.5 h;
参考文献
Russian Chemical Bulletin, , vol. 42, # 4 p. 706 - 708
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 742 - 743
参考文献
Proceedings of the Royal Society of London, Series B: Biological Sciences, , vol. 133, p. 20,30
反应条件
potassium carbonate; palladium dichloride in 1-methyl-pyrrolidin-2-one T=95°C; 7 h;
参考文献
Ryu, Hyung-Chul; Hong, Young-Taek; Kang, Suk-Ku
Heterocycles, 2001 , vol. 54, # 2 p. 985 - 988
反应条件
benzotriazol-1-ol; dicyclohexyl-carbodiimide in N,N-dimethyl-formamide T=20 - 100°C; 20 h;
参考文献
Ono, Masahiro; Haratake, Mamoru; Saji, Hideo; Nakayama, Morio
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 14 p. 6867 - 6872
反应条件
T=140°C; 0.0333333 h; Microwave irradiationSealed vessel;
参考文献
Neves Filho, Ricardo Antonio Wanderley; Da Silva, Cecilia Aguiar; Da Silva, Clecia Sipriano Borges; Brustein, Vanessa Passos; Navarro, Daniela Maria Do Amaral Ferraz; Dos Santos, Fabio Andre Brayner; Alves, Luiz Carlos; Cavalcanti, Marilia Gabriela Dos Santos; Srivastava, Rajendra Mohan; Carneiro-Da-Cunha, Maria Das Gracas
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 8 p. 819 - 825
参考文献
Srivastava; Borges Viana de; Bieber
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 4 p. 1193 - 1195
反应条件
in tetrahydrofuran 4.5 h; Heating;
参考文献
Dos Santos Filho, Jose Mauricio; Moreira, Diogo Rodrigo M.; De Simone, Carlos Alberto; Ferreira, Rafaela Salgado; McKerrow, James H.; Meira, Cassio Santana; Guimaraes, Elisalva Teixeira; Soares, Milena Botelho Pereira
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 21 p. 6423 - 6433,11
反应条件
potassium carbonate; palladium dichloride in 1-methyl-pyrrolidin-2-one T=95°C; 7 h;
参考文献
Ryu, Hyung-Chul; Hong, Young-Taek; Kang, Suk-Ku
Heterocycles, 2001 , vol. 54, # 2 p. 985 - 988
