2-苯基-2H-苯并噻唑合成路线 （共 42 条）
参考文献
Gattermann; Wichmann
Chemische Berichte, 1888 , vol. 21, p. 1636
反应条件
sodium hydroxide; sodium thiosulfate in ethanol
T=60°C; Heating / reflux;
参考文献
CIBA CORPORATION
Patent: US2009/62560 A1, 2009 ;
Location in patent: Page/Page column 31-32 ;
反应条件
in dimethyl sulfoxide
T=125°C; 10 h;
参考文献
Fischer, Walter; Fritzsche, Katharina; Wolf, Walter; Bore, Lothar
Patent: US2004/19220 A1, 2004 ;
Location in patent: Page 9 ;
反应条件
pyridine; oxygen; copper(l) chloride
T=20°C; 0.166667 h;
参考文献
Terpugova, M. P.; Amosov, Yu. I.; Kotlyarevskii, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 5 p. 1040 - 1042
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 5 p. 1166 - 1168
反应条件
cesium fluoride in acetonitrile
T=20°C; 24 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
T=120°C; 5 h; Inert atmosphereSchlenk technique;
参考文献
Tian, Qingshan; Chen, Xianmin; Liu, Wei; Wang, Zechao; Shi, Suping; Kuang, Chunxiang
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7830 - 7833
反应条件
copper(l) iodide; sodium azide; N,N,N',N,-tetramethylethylenediamine; N-hexadecyl-N,N,N-trimethylammonium bromide in water
T=130°C; 16 h; Sealed tubeInert atmosphere;
参考文献
Shang, Xiaobo; Zhao, Shixian; Chen, Wanzhi; Chen, Chao; Qiu, Huayu
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1825 - 1828
反应条件
copper(l) iodide; sodium azide; N,N,N',N,-tetramethylethylenediamine; N-hexadecyl-N,N,N-trimethylammonium bromide in water
T=130°C; 16 h; Sealed tubeInert atmosphere;
参考文献
Shang, Xiaobo; Zhao, Shixian; Chen, Wanzhi; Chen, Chao; Qiu, Huayu
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1825 - 1828
反应条件
sodium hydroxide; hydroxylamine hydrochloride in ethanol
T=85 - 90°C; 0.5 h;
参考文献
Wilshire, John F.K.
Australian Journal of Chemistry, 1988 , vol. 41, # 4 p. 617 - 622
反应条件
in melt
T=145°C; 0.0833333 h;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
