1: ω-Hydroxyundecyl triphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane T=-15°C; 2 h; 2: propionaldehyde in tetrahydrofuran; hexane T=-15 - 20°C; 3: acetic anhydride With pyridine T=20°C; 15 h; Further stages. Title compound not separated from byproducts.;
参考文献
Li; Yong; Aisa
Chemistry of Natural Compounds, 2008 , vol. 44, # 2 p. 224 - 226
