4,4’-双叔丁基二苯基甲烷合成路线 (共 28 条)
反应条件
aluminium trichloride; nitromethane
参考文献
Yamato, Takehiko; Sakaue, Naozumi; Furusawa, Takashi; Tashiro, Masahi; Prakash, G.K.Surya; Olah, George A.
Journal of Chemical Research, Miniprint, 1991 , # 9 p. 2414 - 2438
反应条件
AlCl3, aluminium chloride T=20°C; Product distribution / selectivity;
参考文献
Lebedev, Artyom Vuryevich; Asachenko, Andrel Fyodorovich; Voskoboynikov, Alexander Zelmanovich; Razavi, Abbas
Patent: US2011/9683 A1, 2011 ;
Location in patent: Page/Page column 2 ;
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in water; N,N-dimethyl-formamide T=153°C; 12 h;
参考文献
Wang, Xing; Liu, Lian-Hua; Shi, Jin-Hua; Peng, Ji; Tu, Hai-Yang; Zhang, Ai-Dong
European Journal of Organic Chemistry, 2013 , # 30 p. 6870 - 6877
反应条件
1: 1-bromo-4-(1,1-dimethylethyl)benzene With iodine; magnesium in tetrahydrofuran Metallation; 12 h; Heating; 2: 1,1-dibromomethane With copper(I) bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Grignard reaction; 2 h; Heating;
参考文献
Yamato, Takehiko; Sakaue, Naozumi; Suehiro, Kazuaki; Tashiro, Masashi
Organic Preparations and Procedures International, 1991 , vol. 23, # 5 p. 617 - 620
反应条件
potassium hydroxide; Raney Ni-Al alloy in water T=90°C; 9 h;
参考文献
Liu, Guo-Bin; Zhao, Hong-Yun; Zhu, Jia-Da; He, Hong-Jie; Yang, Hong-Jie; Thiemann, Thies; Tashiro, Hideki; Tashiro, Masashi
Synthetic Communications, 2008 , vol. 38, # 10 p. 1651 - 1661
反应条件
methanesulfonic acid; phosphorus pentoxide 24 h; Ambient temperature;
参考文献
Yonezawa, Noriyuki; Hino, Tetsuo; Tokita, Yoshimi; Matsuda, Kazuhisa; Ikeda, Tomiki
Tetrahedron, 1997 , vol. 53, # 42 p. 14287 - 14296
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 34, # 3 p. 280 - 284,38 - 40
反应条件
in tetrahydrofuran T=30°C; Equilibrium constant;
参考文献
Tetrahedron, , vol. 42, # 17 p. 4729 - 4742
反应条件
in tetrahydrofuran T=30°C; Equilibrium constant;
参考文献
Tetrahedron, , vol. 42, # 17 p. 4729 - 4742
反应条件
in tetrahydrofuran T=30°C; Equilibrium constant;
参考文献
Tetrahedron, , vol. 42, # 17 p. 4729 - 4742