(4-氯苯基)甲基4-氯苯甲酸酯合成路线 (共 17 条)
反应条件
C42H36ClIrO2P2; caesium carbonate in para-xylene
36 h; Inert atmosphereReflux;
参考文献
Musa, Sanaa; Shaposhnikov, Irina; Cohen, Shmuel; Gelman, Dmitri
Angewandte Chemie - International Edition, 2011 , vol. 50, # 15 p. 3533 - 3537
反应条件
2,4,6-trimethyl-pyridine; hydrogen; chlorohydridotris(triphenylphosphine)ruthenium in toluene
T=55°C; P=760 Torr; 15 h; or (Ph3P)3RuCl2, 20 h;
参考文献
Grushin, Vladimir V.; Alper, Howard
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5159 - 5161
反应条件
Me2SiCp''2Th(n-C4H9) in benzene-d6
T=25°C; Tishchenko reaction; 24 h; chemoselective reaction;
参考文献
Li, Jie; Shi, Jingchao; Han, Hongfei; Guo, Zhiqiang; Tong, Hongbo; Wei, Xuehong; Liu, Diansheng; Lappert, Michael F.
Organometallics, 2013 , vol. 32, # 13 p. 3721 - 3727
反应条件
La[N(TMS)2]3 in benzene-d6
T=25°C; 24 h;
参考文献
Seo, SungYong; Marks, Tobin J.
Organic Letters, 2008 , vol. 10, # 2 p. 317 - 319
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water
T=80°C; 6 h;
参考文献
Majji, Ganesh; Guin, Srimanta; Gogoi, Anupal; Rout, Saroj Kumar; Patel, Bhisma K.
Chemical Communications, 2013 , vol. 49, # 29 p. 3031 - 3033
反应条件
18-crown-6 ether; oxygen; potassium carbonate in tetrahydrofuran; water
T=70°C; P=760.051 Torr; 24 h;
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
cerium; mercury in tetrahydrofuran
T=0°C; 2 h;
参考文献
Imamoto, Tsuneo; Kusumoto, Tetsuo; Tawarayama, Yoshinori; Sugiura, Yasushi; Mita, Takeshi; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3904 - 3912
反应条件
4-(N,N-dimethlyamino)pyridine; oxygen; benzyl bromide in acetonitrile
T=180°C; P=7500.75 Torr; 3 h; Autoclave;
参考文献
Zhang, Zhan; Gao, Jin; Wang, Feng; Xu, Jie
Molecules, 2012 , vol. 17, # 4 p. 3957 - 3968
反应条件
trimethylamine borane in xylene
9 h; Heating;
参考文献
Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea; Liso, Gaetano
Synthesis, 1990 , # 9 p. 853 - 854
反应条件
EtNdI in tetrahydrofuran
T=65°C; 20 h;
参考文献
Yokoo, Kazuhiro; Mine, Norioko; Taniguchi, Hiroshi; Fujiwara, Yuzo
Journal of Organometallic Chemistry, 1985 , vol. 279, p. C19 - C21