2,2,2-三氟-N-辛基乙酰胺合成路线 （共 22 条）
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=50°C; 24 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
boric acid in toluene 20.5 h; Heating / reflux;
参考文献
MIMOS BERHAD
Patent: WO2009/75561 A2, 2009 ;
Location in patent: Page/Page column 9-10 ;
反应条件
trifluoromethyl amino ketone; sodium hydride in N,N-dimethyl-formamide T=80°C; 18 h; Yields of byproduct given;
参考文献
Harland, Philip A.; Hodge, Philip; Maughan, Wilfrid; Wildsmith, Eric
Synthesis, 1984 , # 11 p. 941 - 943
反应条件
trifluoromethyl amino ketone; sodium hydride in N,N-dimethyl-formamide T=80°C; 18 h; Yields of byproduct given;
参考文献
Harland, Philip A.; Hodge, Philip; Maughan, Wilfrid; Wildsmith, Eric
Synthesis, 1984 , # 11 p. 941 - 943
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
trifluoromethyl amino ketone; sodium hydride in N,N-dimethyl-formamide T=80°C; 18 h; Yields of byproduct given;
参考文献
Harland, Philip A.; Hodge, Philip; Maughan, Wilfrid; Wildsmith, Eric
Synthesis, 1984 , # 11 p. 941 - 943
参考文献
Pailer,M.; Huebsch,W.J.
Monatshefte fuer Chemie, 1966 , vol. 97, p. 1541 - 1553
反应条件
sodium hydride 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Harland, Philip A.; Hodge, Philip; Maughan, Wilfrid; Wildsmith, Eric
Synthesis, 1984 , # 11 p. 941 - 943
反应条件
sodium hydride 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Harland, Philip A.; Hodge, Philip; Maughan, Wilfrid; Wildsmith, Eric
Synthesis, 1984 , # 11 p. 941 - 943
