(3,5-二甲氧基苯基)乙酮合成路线 （共 11 条）
反应条件
in diethyl ether T=-78°C; 1 h;
参考文献
Majetich, George; Liu, Shuang; Fang, Jing; Siesel, David; Zhang, Yong
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6928 - 6951
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; 2-methoxy-6-(N-methyl-N-phenyl-amino)phenyl(dicyclohexyl)phosphine; caesium carbonate T=90°C; 12 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Li, Pengbin; Lue, Bo; Fu, Chunling; Ma, Shengming
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 7 p. 1255 - 1259
反应条件
iron; acetic acid 3 h; Heating;
参考文献
Upender; Pollart; Liu; Hobbs; Olsen; Chao; Bowden; Crase; Thomas; Pandey; Lawson; Dawson
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1371 - 1385
反应条件
1: 93 percent / oxalyl chloride / benzene / 17 h / Ambient temperature 2: 64 percent / diethyl ether / 1 h / -78 °C View Scheme
参考文献
Chatterjea, J. N.; Bhakta, C.; Mukherjee, Sanat K.
Journal of the Indian Chemical Society, 1981 , vol. 58, p. 888 - 890
反应条件
1: 62 percent / NH4OAc / 16 h / 100 °C 2: 90 percent / Fe, glacial AcOH / 3 h / Heating View Scheme
参考文献
Hoye, Thomas R.; Chen, Minzhang; Mi, Liang; Priest, Owen P.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8747 - 8750
反应条件
potassium tert-butylate in ammonia Irradiation;
参考文献
Bunnett,J.F.; Sundberg,J.E.
Chemical and Pharmaceutical Bulletin, 1975 , vol. 23, p. 2620 - 2628
参考文献
Birch; Donovan
Australian Journal of Chemistry, 1953 , vol. 6, p. 373
参考文献
Birch; Donovan
Australian Journal of Chemistry, 1953 , vol. 6, p. 373
反应条件
sulfuric acid; magnesium; acetic acid 1.) ether, CCl4, 3 h, reflux; 2.) ether, CCl4, 2 h, reflux; 3.) water, reflux, 5 h; Yield given. Multistep reaction;
参考文献
Chatterjea, J. N.; Bhakta, C.; Mukherjee, Sanat K.
Journal of the Indian Chemical Society, 1981 , vol. 58, p. 888 - 890
反应条件
potassium hydroxide in ethanol
参考文献
Wasserman, Harry H.; Gambale, Ronald J.; Pulwer, Mitchell J.
Tetrahedron, 1981 , vol. 37, # 23 p. 4059 - 4067
