CO in n-heptane
Fe(CO)5 (72 mg, 0.36 mmol) added to a heptane solution (20 ml) of (η3-CPh3)Re(CO)4 (100 mg, 0.18 mmol), the solution was degassed and left under CO (20 psi) for 4 h without stirring;; detected by MS, IR and elem. anal,;;
参考文献
Crocker, Lisa S.; Mattson, Bruce M.; Heinekey, D. Michael; Schulte, Gayle K.
Inorganic Chemistry, 1988 , vol. 27, p. 3722 - 3725
DPDC in benzene
T=60°C; 5 h; Further byproducts given;
参考文献
Leardini, Rino; Nanni, Daniele; Pedulli, Gian Franco; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1591 - 1594
