3,4,5-三甲氧基苯甲腈合成路线 （共 50 条）
反应条件
DMEG; triethylamine in dichloromethane T=20°C; Dehydration; 18 h;
参考文献
Isobe, Toshio; Ishikawa, Tsutomu
Journal of Organic Chemistry, 1999 , vol. 64, # 19 p. 6984 - 6988
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78°C; 1.5 h; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
hydroxylamine hydrochloride in 1-methyl-pyrrolidin-2-one T=100°C; 0.5 h;
参考文献
Chakraborti; Kaur; Roy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1000 - 1006
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78°C; 1.5 h; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
tert.-butylhydroperoxide; copper(l) iodide in N,N-dimethyl acetamide; water T=130°C; 20 h;
参考文献
Luo, Yan; Wen, Qiaodong; Wu, Zhiyuan; Jin, Jisong; Lu, Ping; Wang, Yanguang
Tetrahedron, 2013 , vol. 69, # 39 p. 8400 - 8404
反应条件
1: With sodium diisobutyl-tert-butoxyaluminium hydride in tetrahydrofuran T=0°C; 4 h; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; water T=0 - 20°C; 3 h;
参考文献
Suzuki, Yusuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 41 p. 7956 - 7962
反应条件
dihydrogen peroxide; o-nitrobenzeneseleninic acid in methanol T=20°C; 36 h;
参考文献
Said, Samy Bayomy; Skarzewski, Jacek; Mlochowski, Jacek
Synthesis, 1989 , # 3 p. 223 - 224
反应条件
triethylamine; 2,2,2-trichloroacetyl chloride in dichloromethane
参考文献
Saednya, Akbar
Synthesis, 1985 , # 2 p. 184 - 185
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tert.-butylhydroperoxide; potassium iodide in water T=20°C; 4 h;
参考文献
Lamani, Manjunath; Devadig, Pradeep; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 14 p. 2753 - 2759
反应条件
sodium azide; N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane; dimethyl sulfoxide T=0 - 20°C; 4 h;
参考文献
Kangani, Cyrous O.; Day, Billy W.; Kelley, David E.
Tetrahedron Letters, 2008 , vol. 49, # 5 p. 914 - 918
