5-甲氧基-2-硝基苯甲酸合成路线 (共 47 条)
反应条件
ethanol; iron; ammonium chloride
参考文献
National Science Council
Patent: US6479499 B1, 2002 ;
US 6479499 B1
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
KIRIN BEER KABUSHIKI KAISHA
Patent: EP1724268 A1, 2006 ;
Location in patent: Page/Page column 49 ;
反应条件
hydrogenchloride in water T=0 - 20°C; 22 h; Heating / reflux;
参考文献
PFIZER LIMITED; PFIZER INC.
Patent: WO2005/121152 A1, 2005 ;
Location in patent: Page/Page column 30 ;
WO 2005/121152 A1
反应条件
in methanol; dichloromethane T=20°C; 10 h;
参考文献
MERCK and CO., INC.
Patent: WO2006/52555 A2, 2006 ;
Location in patent: Page/Page column 35; 82-83 ;
反应条件
copper quinolate in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
参考文献
Sevbo, D. P.; Stepanova, T. F.; Nekhoroshev, A. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1097 - 1101
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1268 - 1274
参考文献
Morrison; Mulholland
Journal of the Chemical Society, 1958 , p. 2702,2703
反应条件
pyridine hydrochloride T=150°C; 3 h;
参考文献
Vialaton, Delphine; Baglio, Daniela; Paya-Perez, Ana; Richard, Claire
Pest Management Science, 2001 , vol. 57, # 4 p. 372 - 379
反应条件
in water pH=12; Photolysis; Quantum yieldProduct distribution; Further Variations:pH-values;
参考文献
Vialaton, Delphine; Baglio, Daniela; Paya-Perez, Ana; Richard, Claire
Pest Management Science, 2001 , vol. 57, # 4 p. 372 - 379
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 24 h;
参考文献
Marks, Andrew R.; Landry, Donald W.; Deng, Shi Xian; Cheng, Zhen Zhuang
Patent: US2005/215540 A1, 2005 ;
Location in patent: Page/Page column 37 ;