1: benzenesulphinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide T=20°C; 6 h; solid-phase reaction; 2: acrylic acid methyl ester With 2,2'-azo-bisisobutyronitrile in benzene 20 h; Heating; 3: With dihydrogen peroxide in tetrahydrofuran T=20°C; 2 h;
in tetrahydrofuran To a stirred soln. of complex in THF was added dropwise a soln. of ligand in THF at -20°C., the soln. was stirred for ca. 1 h (Ar atm.);; recrystd. from Et2O-THF at -20°C; elem. anal.;;
参考文献
Buech, H. Michael; Binger, Paul; Krueger, Garl
Organometallics, 1984 , vol. 3, p. 1504 - 1509
