2-[(2-溴苯甲酰基)氨基]苯甲酸合成路线 (共 5 条)
反应条件
sodium hydroxide in methanol; water
T=80°C; 3 h; Inert atmosphere;
参考文献
Shen, Zengming; Ni, Zhenjie; Mo, Song; Wang, Jing; Zhu, Yamin
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4859 - 4865
反应条件
1: pyridine
2: aq. NaOH
View Scheme
参考文献
Bain,D.I.; Smalley,R.K.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 1593 - 1597
反应条件
1: pyridine
2: aq. NaOH
View Scheme
参考文献
Bain,D.I.; Smalley,R.K.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 1593 - 1597
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice
2: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
3: sodium hydroxide / methanol; water / 3 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Shen, Zengming; Ni, Zhenjie; Mo, Song; Wang, Jing; Zhu, Yamin
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4859 - 4865
参考文献
Bain,D.I.; Smalley,R.K.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 1593 - 1597