Iglesias, Rodrigo S.; Claessens, Christian G.; Torres, Tomas; Herranz, M. Angeles; Ferro, Victor R.; Garcia De La Vega, Jose M.
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 2967 - 2977
in further solvent(s)
N2-atmosphere, 25percentstoich. excess of tetrafluorophthalonitrile, refluxing in 1-chloronaphtalene (24 h); cooling to room temp., filtration, addn. of petroleum ether, cooling in ice bath (pptn.), filtration, recrystn. (H2SO4);
参考文献
Balkus, Kenneth J.; Gabrielov, Alexei G.; Bell, Stephen L.; Bedioui, Fethi; Roue, Lionel; Devynck, Jacques
Inorganic Chemistry, 1994 , vol. 33, p. 67 - 72