2-(三甲基硅氧基)丙烯合成路线 (共 98 条)
参考文献
Journal of Organometallic Chemistry, , vol. 66, p. 29 - 41
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 48, # 8 p. 1738 - 1742,1587 - 1590
参考文献
Journal of Organometallic Chemistry, , vol. 3, p. 478
Zhurnal Obshchei Khimii, , vol. 36, p. 158 - 158
Zhurnal Obshchei Khimii, , vol. 36, p. 153 - 157
Zhurnal Obshchei Khimii, , vol. 35, p. 760 - 760
Zhurnal Obshchei Khimii, , vol. 35, p. 757 - 758
参考文献
Journal of Organometallic Chemistry, , vol. 3, p. 478
Zhurnal Obshchei Khimii, , vol. 36, p. 158 - 158
Zhurnal Obshchei Khimii, , vol. 36, p. 153 - 157
Zhurnal Obshchei Khimii, , vol. 35, p. 760 - 760
Zhurnal Obshchei Khimii, , vol. 35, p. 757 - 758
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 36, # 1 p. 153 - 157,158 - 161
反应条件
trifluorormethanesulfonic acid in diethyl ether; dichloromethane T=-20°C; 3 h; Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Ziegler, Thomas; Schoenwaelder, Karl-Heinz; Kesmarszky, Thomas; Bauer, Bernd
Chemische Berichte, 1986 , vol. 119, # 11 p. 3394 - 3404
反应条件
titanium tetrachloride Mukaiyama Reaction;
参考文献
NORTH CAROLINA STATE UNIVERSITY
Patent: WO2007/64842 A2, 2007 ;
Location in patent: Page/Page column 124 ;
反应条件
tetrabutyl ammonium fluoride; fluorine 1.) CH2Cl2, not above -50 deg C, 2.) CH2Cl2, a) -50 deg C, 1 h, b) -50 to 0 deg C, 1 h, c) 0 deg C, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kiselyov, Alexander S.; Strekowski, Lucjan
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4476 - 4478
反应条件
zinc(II) chloride in ethyl acetate T=20 - 25°C; 2 h;
参考文献
Makin, S. M.; Kruglikova, R. I.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 630 - 634
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 723 - 727
反应条件
[Ir(cod)(PPh3)2]OTf; hydrogen in dichloromethane T=25°C; crossed aldol coupling; desilylation; 3 h;
参考文献
Matsuda, Isamu; Hasegawa, Yuki; Makino, Tatsuya; Itoh, Kenji
Tetrahedron Letters, 2000 , vol. 41, # 9 p. 1405 - 1408