2,4,2',4'-四硝基联苯合成路线 （共 14 条）
反应条件
copper; bis(dibenzylideneacetone)-palladium(0) in dimethyl sulfoxide
T=70°C; Ullmann cross-coupling; 1 h;
参考文献
Banwell, Martin G.; Kelly, Brian D.; Kokas, Okanya J.; Lupton, David W.
Organic Letters, 2003 , vol. 5, # 14 p. 2497 - 2500
反应条件
sulfuric acid; nitric acid
T=100°C; 20 h;
参考文献
Cornforth, John; Sierakowski, Andrew F.; Wallace Timothy W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2299 - 2316
反应条件
sulfuric acid; nitric acid
T=110°C; 6 h;
参考文献
Adrievskii, A. M.; Poplavskii, A. N.; Dyumaev, K. M.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1195 - 1198
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1314 - 1317
反应条件
copper; nitrobenzene
参考文献
Ullmann; Bielecki
Chemische Berichte, 1901 , vol. 34, p. 2176
反应条件
sulfuric acid; nitric acid
T=100 - 120°C;
参考文献
Swann Research Inc.
Patent: US1870627 , 1930 ;
反应条件
sulfuric acid; nitric acid
T=100 - 120°C;
参考文献
Swann Research Inc.
Patent: US1870627 , 1930 ;
反应条件
lithium alcoholate of 5-hydroxymethyl-3-methyl-5-nitro-1,3-tetrahydrooxazine in dimethyl sulfoxide
参考文献
Galeeva, A. G.; Trifonova, V. N.; Kasatkina, A. A.; Zorin, V. V.; Rakhmankulov, D. L.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 6.2 p. 1019 - 1021
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 6 p. 1228 - 1230
参考文献
Forrest,J.
Journal of the Chemical Society, 1960 , p. 594 - 601
反应条件
sulfuric acid; nitric acid
T=160°C; 2 h; Further byproducts given;
参考文献
Adrievskii, A. M.; Poplavskii, A. N.; Dyumaev, K. M.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1195 - 1198
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1314 - 1317
反应条件
sulfuric acid; nitric acid
T=250°C; 1 h; Further byproducts given;
参考文献
Adrievskii, A. M.; Poplavskii, A. N.; Dyumaev, K. M.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1195 - 1198
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1314 - 1317
