4,4'-二硝基二苯基甲烷合成路线 （共 39 条）
反应条件
tetramethyl-ammonium fluoride; dimethyl sulfoxide T=100°C; 1 h; Yield given;
参考文献
Adams, Dave J.; Clark, James H.; McFarland, Heather
Journal of Fluorine Chemistry, 1998 , vol. 92, # 2 p. 127 - 129
反应条件
1: NaHS; aqueous ethanol 2: Raney nickel; methanol; N2H4+H2O View Scheme
参考文献
Litwinenko et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1470,1472; engl. Ausg. S. 1444, 1445
反应条件
sodium hydrogensulfide; ethanol
参考文献
Litwinenko et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1470,1472; engl. Ausg. S. 1444, 1445
参考文献
Litwinenko et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1470,1472; engl. Ausg. S. 1444, 1445
反应条件
1: With sodium hydride in tetrahydrofuran T=0°C; 1 h; Inert atmosphere; 2: With 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in tetrahydrofuran; N,N-dimethyl-formamide T=0°C;
参考文献
Kamlar, Martin; Putaj, Piotr; Vesely, Jan
Tetrahedron Letters, 2013 , vol. 54, # 16 p. 2097 - 2100
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran; water T=20°C; 0.5 h;
参考文献
Organic Letters, , vol. 7, # 22 p. 5087 - 5090
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Synthesis, , # 19 p. 3316 - 3340
参考文献
Justus Liebigs Annalen der Chemie, , vol. 283, p. 157
Chemische Berichte, , vol. 5, p. 796
反应条件
sulfuric acid; nitric acid T=120 - 140°C; 3 h;
参考文献
Jarczewski, Arnold; Schroeder, Grzegorz; Leffek, Kenneth T.
Canadian Journal of Chemistry, 1991 , vol. 69, # 3 p. 468 - 473
反应条件
1: Ag2SO4; H2SO4; chlorine
2: SnCl2; concentrated aqueous HCl
View Scheme
参考文献
Gorvin
Journal of the Chemical Society, 1955 , p. 83,86
