1-烯丙基-4-(三氟甲基)苯合成路线 （共 13 条）
反应条件
pyridine; manganese; FeBr2; cobalt(II) dibromide in acetonitrile T=50°C; 24 h;
参考文献
Organic Letters, , vol. 5, # 7 p. 1043 - 1045
反应条件
1: ethylene,methyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: 4-trifluoromethyl-1-iodobenzene in N,N-dimethyl-formamide T=100°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1641 - 1645
反应条件
bromobenzene; zinc dibromide; zinc; acetic acid; cobalt(II) dibromide in acetonitrile T=20°C; 3 h;
参考文献
Organic Letters, , vol. 5, # 7 p. 1043 - 1045
反应条件
pyridine; tetrabutyl ammonium fluoride; cobalt(II) dibromide T=50°C; Electrolysis;
参考文献
Gomes, Paulo; Gosmini, Corinne; Perichon, Jacques
Journal of Organic Chemistry, 2003 , vol. 68, # 3 p. 1142 - 1145
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=70°C; i = 250 mA, nickel-sponge cathode;
参考文献
Durandetti, Muriel; Nedelec, Jean-Yves; Perichon, Jacques
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1748 - 1755
反应条件
triphenyl phosphite; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Kayaki, Yoshihito; Koda, Takashi; Ikariya, Takao
European Journal of Organic Chemistry, 2004 , # 24 p. 4989 - 4993
反应条件
diisobutylaluminium hydride; bis(acetylacetonate)nickel(II); triphenylphosphine in ethylene glycol dimethyl ether; hexane T=80°C; 3 h;
参考文献
Shirakawa, Eiji; Yamasaki, Kenji; Hiyama, Tamejiro
Synthesis, 1998 , # 10 p. 1544 - 1549
反应条件
in diethyl ether 48 h; Ambient temperature;
参考文献
Di Benedetto, Silvia; Consiglio, Giambattista
Helvetica Chimica Acta, 1997 , vol. 80, # 7 p. 2204 - 2214
反应条件
C48H32As2Br2F10Pd2; p-benozquinone in chloroform T=50°C; Stille coupling; 24 h; Inert atmosphere;
参考文献
Carrera, Nora; Gutierrez, Enrique; Benavente, Rut; Villavieja, M. Mar; Albeniz, Ana C.; Espinet, Pablo
Chemistry - A European Journal, 2008 , vol. 14, # 32 p. 10141 - 10148
反应条件
1: Mg / diethyl ether 2: 60 percent / diethyl ether / 48 h / Ambient temperature View Scheme
参考文献
Helvetica Chimica Acta, , vol. 80, # 7 p. 2204 - 2214
