1H-茚-1-基三甲基硅烷合成路线 （共 14 条）
反应条件
H2SO4 in sulfuric acid byproducts: indene; aq. H2SO4; varoius concs. of H2SO4; various temp.;;
参考文献
Sommer, L. H.; Marans, N. S.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135 - 5138
反应条件
in dichloromethane to TiCl4 in CH2Cl2, indene deriv. in CH2Cl2 added dropwise at 0°C; mixt. stirred overnight at room temp.; solvent removed under vac.; to residue, hexane added; suspn. cooled to -30°C for several h; ppt. collected by filtration; washed with cold hexane; dried under vac.;
参考文献
Weiss; Voelkening; Rueffer; Meichel; Sachse; Rheinwald; Lang
Zeitschrift fur Anorganische und Allgemeine Chemie, 2007 , vol. 633, # 13-14 p. 2242 - 2254
反应条件
n-butyllithium in hexane
参考文献
The Dow Chemical Company
Patent: US4962253 A1, 1990 ;
参考文献
Gmelin Handbook: Si: MVol.C, 29, page 90 - 93
