1,4-二甲基-9H-咔唑合成路线 （共 61 条）
反应条件
trichlorophosphate in toluene T=111°C; 6.5 h;
参考文献
Deane, Fiona M.; Miller, Charlotte M.; Maguire, Anita R.; McCarthy, Florence O.
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 4 p. 814 - 823
反应条件
in dichloromethane 4.5 h; -78 deg C to room temperature; Yields of byproduct given;
参考文献
Flo, Camran; Pindur, Ulf
Liebigs Annalen der Chemie, 1987 , p. 509 - 514
反应条件
montmorillonite K-10
T=90°C; 0.2 h; microwave heating;
参考文献
Abid, Mohammed; Spaeth, Andrew; Toeroek, Bela
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 15 p. 2191 - 2196
反应条件
palladium diacetate; sodium t-butanolate; [(t-Bu)3PH]BF4 in toluene
T=160°C; 3 h; microwave irradiation;
参考文献
Bedford, Robin B.; Betham, Michael
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9403 - 9410
反应条件
bicyclo-[2.2.1]hept-2-ene; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=105°C; 48 h; Inert atmosphere;
参考文献
Della Ca', Nicola; Sassi, Giovanni; Catellani, Marta
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 14-15 p. 2179 - 2182
反应条件
palladium on activated charcoal in various solvent(s)
参考文献
Mustafin; Khalilov; Sharafutdinov; D'yachenko; Abdrakhmanov; Tolstikov
Russian Chemical Bulletin, 1997 , vol. 46, # 3 p. 608 - 609
反应条件
aluminium trichloride in benzene
T=20°C; 4 h;
参考文献
Kikugawa; Aoki; Sakamoto
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8612 - 8615
反应条件
palladium on activated charcoal in various solvent(s)
3 h; Heating;
参考文献
Mustafin, A. G.; Khalilov, I. N.; Abdakhmanov, I. B.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1989 , vol. 25, # 6 p. 693 - 695
Khimiya Prirodnykh Soedinenii, 1989 , # 6 p. 816 - 818
反应条件
sulfuric acid; silica gel in dichloromethane
120 h;
参考文献
Deane, Fiona M.; Miller, Charlotte M.; Maguire, Anita R.; McCarthy, Florence O.
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 4 p. 814 - 823
反应条件
cesium fluoride in acetonitrile
T=20°C;
参考文献
Chakrabarty, Shyamal; Chatterjee, Indranil; Tebben, Ludger; Studer, Armido
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2968 - 2971
Angew. Chem., 2013 , vol. 125, # 10 p. 3041 - 3044
