三(三甲代甲硅烷基)亚磷酸盐合成路线 （共 38 条）
反应条件
orthophosphorus acid 2 h; Heating;
参考文献
Synthetic Communications, , vol. 34, # 6 p. 1017 - 1022
参考文献
Polish Journal of Chemistry, , vol. 75, # 5 p. 663 - 672
反应条件
in dichloromethane var. alkyl trimethylsilyl phosphites; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 215, # 3 p. 355 - 365
反应条件
methanol 1.) 130 deg C, 5 h, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Serves, Spyros V.; Sotiropoulos, Demetrios N.; Ioannou, Panayiotis V.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 107, # 1-4 p. 27 - 32
反应条件
bromine in diethyl ether T=-40 - -30°C; 0.5 h;
参考文献
Michalski, Jan; Pakulski, Marek; Skowronska, Aleksandra
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 833 - 836
反应条件
in pentane T=-15 - 10°C;
参考文献
Mironov, V. F.; Sinyashina, T. N.; Ofitserov, E. N.; Konovalova, I. V.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 7.2 p. 1681 - 1682,1495 - 1496
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 107, # 1-4 p. 27 - 32
反应条件
zinc(II) chloride 1.) C6H6, reflux, 5 min; 2.) room temp., 40 h; Yield given. Multistep reaction;
参考文献
Huber, Rolf; Vasella, Andrea
Helvetica Chimica Acta, 1987 , vol. 70, p. 1461 - 1476
反应条件
zinc(II) chloride 1.) C6H6, reflux, 5 min; 2.) room temp., 40 h; Yield given. Multistep reaction;
参考文献
Huber, Rolf; Vasella, Andrea
Helvetica Chimica Acta, 1987 , vol. 70, p. 1461 - 1476
反应条件
in toluene Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
