2-氨基-6-甲氧基吡啶合成路线 （共 12 条）
反应条件
copper(I) oxide; potassium carbonate; ammonium hydroxide; N,N-dimethylethylenediamine in ethylene glycol T=80°C; 16 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 46, # 6 p. 925 - 927
反应条件
dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate in 1,4-dioxane T=50°C; 24 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 14 p. 3734 - 3737
反应条件
methanol; sodium methylate T=170°C;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 1147,1148
反应条件
1: diphenylphosphoryl azide, triethylamine / 26 h / Heating 2: 25percent HBr / 2 h / Ambient temperature 3: methanol / 7 h / 140 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 35, # 10 p. 2025 - 2034
反应条件
1: 25percent HBr / 2 h / Ambient temperature 2: methanol / 7 h / 140 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 35, # 10 p. 2025 - 2034
反应条件
in methanol T=140°C; 7 h;
参考文献
Australian Journal of Chemistry, , vol. 35, # 10 p. 2025 - 2034
反应条件
copper(I) oxide; ammonia T=80°C; 16 h;
参考文献
Tetrahedron Letters, , vol. 42, # 19 p. 3251 - 3254
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0 - 20 °C 2: [Cp*RhCl2]2; silver hexafluoroantimonate; copper diacetate / 1,2-dichloro-ethane / 36 h / 120 °C / |Schlenk technique; |Inert atmosphere 3: palladium 10 on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr 4: hydrogenchloride / water / 6 h / 80 °C View Scheme
参考文献
Zhou, Jun; Li, Bo; Hu, Fang; Shi, Bing-Feng
Organic Letters, 2013 , vol. 15, # 13 p. 3460 - 3463
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C;
参考文献
Zhou, Jun; Li, Bo; Hu, Fang; Shi, Bing-Feng
Organic Letters, 2013 , vol. 15, # 13 p. 3460 - 3463
反应条件
sulfuric acid; potassium nitrate T=75°C; 2 h;
参考文献
Deady, Leslie W.; Korytsky, Olga L.; Rowe, Jeffrey E.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2025 - 2034
