1,3-双(三甲基硅氧基)丙烷合成路线 （共 27 条）
反应条件
iodine in dichloromethane T=20°C; 65 h;
参考文献
Karimi, Babak; Golshani, Behzad
Synthesis, 2002 , # 6 p. 784 - 788
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 12 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 6.5 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 15 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
in dichloromethane
under N2, freshly distd. 2-phenylpropene added dropwise to CH2Cl2 soln.of BHBr2*SMe2 with water bath (15°C), cooled, mixt. left overnight at room temp., 1,3-bis(trimethylsiloxy)propane added, stirred for 3 h; solvent and volatiles removed by aspirator vac.;
参考文献
Brown; Imai
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6285 - 6289
反应条件
iodine in dichloromethane
T=20°C; 66 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 168 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
1: in toluene
T=-78°C; 0.166667 h;
2: With iron chloride in toluene
T=-40°C; 12 h;
参考文献
Tsukada, Hiroyuki; Mukaeda, Yuki; Hosokawa, Seijiro
Organic Letters, 2013 , vol. 15, # 3 p. 678 - 681
反应条件
iodine in dichloromethane
T=20°C; 27.5 h;
参考文献
Karimi, Babak; Golshani, Behzad
Synthesis, 2002 , # 6 p. 784 - 788
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 10 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
