三甲氧基(对甲苯基)硅烷合成路线 (共 43 条)
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=20°C; Hiyama Coupling; 12 h;
参考文献
Journal of Chemical Research, , vol. 38, # 2 p. 123 - 127
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; palladium diacetate in 1,4-dioxane T=80°C; Hiyama cross-coupling reaction; 4 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Liu, Wen-Jie; Xie, Ye-Xiang
Synthesis, 2005 , # 18 art. no. F08405SS, p. 3039 - 3044
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in N,N-dimethyl-formamide; acetonitrile T=100°C; Hiyama Coupling; 3 h; Inert atmosphereGreen chemistry;
参考文献
Zhang, Wei; Liu, Fang; Li, Ke; Zhao, Baoli
Applied Organometallic Chemistry, 2014 , vol. 28, # 5 p. 379 - 381
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
C14H16N6; palladium diacetate; silver fluoride in N,N-dimethyl acetamide
T=60°C; Mizoroki-Heck type reaction; 24 h;
参考文献
Mino, Takashi; Shibuya, Masanori; Suzuki, Saori; Hirai, Kiminori; Sakamoto, Masami; Fujita, Tsutomu
Tetrahedron, 2012 , vol. 68, # 2 p. 429 - 432
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol
T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Zhang, Liang; Qing, Jiang; Yang, Pengyuan; Wu, Jie
Organic Letters, 2008 , vol. 10, # 21 p. 4971 - 4974
反应条件
tBu2P-N=P(iBuPCH2CH2)3N; tetrabutyl ammonium fluoride; palladium diacetate
T=80°C; Hiyama coupling; 3 h; Inert atmosphereNeat (no solvent);
参考文献
Raders, Steven M.; Kingston, Jesudoss V.; Verkade, John G.
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1744 - 1747
反应条件
tetrabutyl ammonium fluoride; tris-(o-tolyl)phosphine; dichloro bis(acetonitrile) palladium(II)
T=80°C; Hiyama cross-coupling reaction; 0.666667 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Xie, Ye-Xiang
Synthesis, 2006 , # 6 p. 969 - 974
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; palladium diacetate in 1,4-dioxane
T=80°C; Hiyama cross-coupling reaction; 4 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Liu, Wen-Jie; Xie, Ye-Xiang
Synthesis, 2005 , # 18 art. no. F08405SS, p. 3039 - 3044
反应条件
CM-phos; tetrabutyl ammonium fluoride; palladium diacetate; acetic acid in tert-butyl alcohol
T=90°C; Hiyama cross-coupling; 16 h; Inert atmosphere;
参考文献
So, Chau Ming; Lee, Hang Wai; Lau, Chak Po; Kwong, Fuk Yee
Organic Letters, 2009 , vol. 11, # 2 p. 317 - 320