1-三甲基甲硅烷基氧基-3-丁炔合成路线 (共 10 条)
反应条件
triethylamine in dichloromethane T=25°C; 1 h;
参考文献
Kedar, Tracey E.; Miller, Michael W.; Hegedus, Louis S.
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6121 - 6126
反应条件
chloro-trimethyl-silane; triethylamine in water; pentane
参考文献
Zoecon Corporation
Patent: US4264518 A1, 1981 ;
反应条件
tris(pentafluorophenyl)-borane in deuterated toluene T=0°C; 1 h; Inert atmosphere;
参考文献
Simonneau, Antoine; Friebel, Jonas; Oestreich, Martin
European Journal of Organic Chemistry, 2014 , vol. 2014, # 10 p. 2077 - 2083
反应条件
in hexane -78 deg C -> r.t., 3 h, reflux;
参考文献
Wrackmeyer, Bernd; Guldner, Gudrun; Abu-Orabi, Sultan T.
Tetrahedron, 1989 , vol. 45, # 4 p. 1119 - 1130
参考文献
Alexakis,A. et al.
Journal of Organometallic Chemistry, 1975 , vol. 96, p. 471 - 485
参考文献
Shostakovskii,M.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, p. 1738 - 1743,1657 - 1661
反应条件
ethylmagnesium bromide in tetrahydrofuran 9 h; Heating;
参考文献
Novokshonov; Medvedeva; Demina; Sherstyannikova; Voronkov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 12 p. 1770 - 1773
参考文献
Curtis, Penelope J.; Davies, Stephen G.
Journal of the Chemical Society, Chemical Communications, 1984 , # 12 p. 747 - 748
反应条件
(i) Cu2Br2, Et2O, (ii) /BRN= 1921566/, pentane, Et2O; Multistep reaction;
参考文献
Alexakis,A. et al.
Journal of Organometallic Chemistry, 1975 , vol. 96, p. 471 - 485
反应条件
hydrogenchloride; copper(I) bromide in dimethylsulfide; hexane; pentane
参考文献
Zoecon Corporation
Patent: US4264518 A1, 1981 ;