1: 1,2-dichloro-1,1,2,2-tetramethyldisilane With pyridine in diethyl ether; water; acetone 1 h; cooling; 2: chloro-trimethyl-silane With triethylamine in diethyl ether; water; acetone 1.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Chernyavskii; Pleshkova
Russian Chemical Bulletin, 2006 , vol. 55, # 4 p. 748 - 750
meta-chloroperoxybenzoic acid in benzene T=35°C; Rate constant;
参考文献
Razuvaev, G. A.; Brevnova, T. N.; Semenov, V. V.; Kornev, A. N.; Lopatin, M. A.; Egorochkin, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 2 p. 375 - 382,323 - 330