1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1.5 h; Inert atmosphere; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=-78 - 20°C; 3: With water in tetrahydrofuran; hexane; ethyl acetate
参考文献
DOW ADVANCED DISPLAY MATERIALS, LTD.; YOON, Seung Soo; KIM, Sung Min; KIM, Bong Ok; KWON, Hyuck Joo; EUM, Sung Jin; CHO, Young Jun; LEE, Hyo Jung
Patent: WO2010/140801 A1, 2010 ;
Location in patent: Page/Page column 18 ;
1: With sodium hydroxide in methanol T=23°C; 0.25 h; 2: With silver trifluoromethanesulfonate in methanol T=0°C; 0.5 h; 3: With 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in hexadeuterioacetone 1 h; Molecular sieve;
参考文献
Brenzovich Jr., William E.; Brazeau, Jean-Francois; Toste, F. Dean
Organic Letters, 2010 , vol. 12, # 21 p. 4728 - 4731
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene T=100°C; 16 h;
参考文献
Garcia-Cuadrado, Domingo; De Mendoza, Paula; Braga, Ataualpa A. C.; Maseras, Feliu; Echavarren, Antonio M.
Journal of the American Chemical Society, 2007 , vol. 129, # 21 p. 6880 - 6886
