1,2,3,4-四氢-2-甲基喹啉合成路线 （共 73 条）
反应条件
C26H29ClIrNO3; hydrogen in 2,2,2-trifluoroethanol T=20°C; P=760.051 Torr; 3 h; TemperatureTimeSolventReagent/catalystPressure;
参考文献
Wu, Jianjun; Barnard, Jonathan H.; Zhang, Yi; Talwar, Dinesh; Robertson, Craig M.; Xiao, Jianliang
Chemical Communications, 2013 , vol. 49, # 63 p. 7052 - 7054
反应条件
palladium 10 on activated carbon; hydrogen in dichloromethane T=20°C; P=912.061 Torr; 3 h;
参考文献
Patti, Angela; Pedotti, Sonia
Tetrahedron, 2010 , vol. 66, # 30 p. 5607 - 5611
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; potassium carbonate in toluene T=111°C; 20 h;
参考文献
Organic Letters, , vol. 4, # 16 p. 2691 - 2694
反应条件
nickel in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Barrero; Alvarez-Manzaneda; Chahboun; Meneses; Romera
Synlett, 2001 , # 4 p. 485 - 488
反应条件
formic acid; triethylamine in dichloromethane
参考文献
EP2733138 A1, ;
Page/Page column ;
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide; water T=20°C; Heck reaction; 0.25 h; 2: 2-iodo aniline With 4'-hydroxyacetophenone oxime palladacycle catalyst in N,N-dimethyl acetamide; water T=120°C; Heck reaction; 8 h; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 17-18 p. 2572 - 2584
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
hydrogen; platinum in trifluoroacetic acid Yield given. Title compound not separated from byproducts;
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Monatshefte fuer Chemie, 1984 , vol. 115, p. 1219 - 1228
反应条件
(R)-(-)-5,5'-bis(diphenylphosphino)-2,2,2',2'-tetrafluoro-4,4'-bi-1,3-benzodioxole; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; hydrogen; iodine in isopropyl alcohol; toluene T=20°C; P=37503.8 Torr; 17 h; Autoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Letters, , vol. 53, # 35 p. 4747 - 4750
