N,N-二甲基-2-苯基硫代乙酰胺合成路线 (共 28 条)
反应条件
Lawesson's reagent in toluene T=100°C; 4 h;
参考文献
Raucher, Stanley; Klein, Peter
Tetrahedron Letters, 1980 , vol. 21, p. 4061 - 4064
反应条件
Na2S*9H2O in N,N-dimethyl-formamide T=80°C; 8 h; Sealed tube;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Li, Jianxiao
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 4 p. 700 - 707
反应条件
sulfur; sodium acetate in N,N-dimethyl-formamide T=100°C; 3 h;
参考文献
Amupitan, Joseph O.
Synthesis, 1983 , # 9 p. 730
反应条件
Na2S*9H2O in N,N-dimethyl-formamide T=80°C; 8 h; Sealed tube;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Li, Jianxiao
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 4 p. 700 - 707
反应条件
sulfur; copper acetylacetonate; pentanal; potassium carbonate T=110°C; 24 h; Schlenk technique;
参考文献
Qu, Yanyang; Li, Zhengkai; Xiang, Haifeng; Zhou, Xiangge
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3141 - 3146
参考文献
Schroth, Werner; Andersch, Joerg
Synthesis, 1989 , # 3 p. 202 - 204
反应条件
in ethylene glycol dimethyl ether 24 h; Ambient temperature;
参考文献
Ogura, Katsuyuki; Ito, Yoko; Tsuchihashi, Gen-ichi
Synthesis, 1980 , # 9 p. 736 - 739
反应条件
boron trifluoride diethyl etherate in diethyl ether 8 h; Ambient temperature;
参考文献
Jong, R.L.P. de; Meijer, J.; Sukhai, R.S.; Bradsma, L.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 9 p. 310 - 313
参考文献
Schroth, Werner; Andersch, Joerg
Synthesis, 1989 , # 3 p. 202 - 204
反应条件
sulfur; triphenylphosphine; cobalt(II) 2,4-pentanedionate T=130°C; 6 h; Yield given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 6.1 p. 1202 - 1206