4-氧杂-1-硫杂螺[4.5]癸烷合成路线 （共 17 条）
反应条件
boron trifluoride diethyl etherate in diethyl ether 3 h; Heating;
参考文献
Chauhan; Kumar, Anil; Sahoo
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 10 p. 2635 - 2637
反应条件
Fe(CF3SO3)3 in acetonitrile T=20°C; 1.5 h;
参考文献
Adibi, Hadi; Jafari, Hadi
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 679 - 682
反应条件
mercury dichloride in dichloromethane 16 h; Ambient temperature;
参考文献
Tanimoto, Shigeo; Jo, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3237 - 3238
反应条件
zinc(II) chloride in dichloromethane 16 h; Ambient temperature;
参考文献
Tanimoto, Shigeo; Jo, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3237 - 3238
反应条件
1: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C 2: conc. aq. HCl / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
1: 30 percent / bis<benzyltriethylammonium> dichromate / hexamethylphosphoric acid triamide / 60 - 80 °C 2: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C 3: conc. aq. HCl / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
hydrogenchloride in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
参考文献
Bergmann et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5662
反应条件
1: in ethanol T=20°C; 2: With water in ethanol T=20°C;
参考文献
Rohman, Md. Rumum; Rajbangshi, Mantu; Laloo, Badaker M.; Sahu, Priti R.; Myrboh, Bekington
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2862 - 2864
反应条件
in tetrahydrofuran 1 h; Ambient temperatureother reaction time; Product distribution;
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1654 - 1657
