1,4-二氧螺环[4,5]癸烷合成路线 （共 57 条）
参考文献
Boeeseken; Tellegen
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 133,141
反应条件
tin(II) trifluoromethanesulfonate; dimethyl tert-butyl silane in acetonitrile
T=0°C;
参考文献
Suzuki, Takeshi; Oriyama, Takeshi
Synthetic Communications, 1999 , vol. 29, # 8 p. 1263 - 1269
反应条件
toluene-4-sulfonic acid in 1,4-dioxane
T=50°C; 1.5 h; Product distribution;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Larionov, V. I.; Zlot-skii, S. S.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1394 - 1401,1229 - 1236
反应条件
water in acetonitrile
2 h; Irradiation;
参考文献
Mella, Mariella; Freccero, Mauro; Albini, Angelo
Journal of Organic Chemistry, 1994 , vol. 59, # 5 p. 1047 - 1052
反应条件
hydrotalcite; Ti(4+) montmorillonite in 1,4-dioxane
T=80°C; 10 h;
参考文献
Motokura, Ken; Fujita, Noriaki; Mori, Kohsuke; Mizugaki, Tomoo; Ebitani, Kohki; Kaneda, Kiyotomi
Journal of the American Chemical Society, 2005 , vol. 127, # 27 p. 9674 - 9675
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
Amberlyst-26
1.) MeOH, 2 h, 2.) THF, room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Cainelli, Gianfranco; Contento, Michele; Manescalchi, Francesco; Regnoli, Rodolfo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2516 - 2519
