1,4-二氧螺环[4,5]癸烷合成路线 （共 57 条）
反应条件
Fe(CF3SO3)3 in acetonitrile T=20°C; 1.5 h;
参考文献
Adibi, Hadi; Jafari, Hadi
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 679 - 682
反应条件
bromine 1.) 0 deg C, 2.) methanol, electrolysis, 2.5 F/mol; Yield given. Multistep reaction;
参考文献
Aben, R.W.M.; Hanneman, E.J.M.; Scheeren, J.W.
Synthetic Communications, 1980 , vol. 10, # 11 p. 821 - 826
反应条件
in acetonitrile 3 h; Irradiation; MechanismQuantum yield;
参考文献
Mella, M.; Fasani, E.; Albini, A.
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3051 - 3057
反应条件
bromine 1.) 0 deg C, 2.) methanol, electrolysis, 2.5 F/mol; Yield given. Multistep reaction;
参考文献
Aben, R.W.M.; Hanneman, E.J.M.; Scheeren, J.W.
Synthetic Communications, 1980 , vol. 10, # 11 p. 821 - 826
反应条件
2,4,6-trichloro-1,3,5-triazine; 1-phenyl-propan-1-one in N,N-dimethyl-formamide T=20°C; 0.75 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
boron trifluoride diethyl etherate; sodium cyanoborohydride in tetrahydrofuran 6 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 51, # 11 p. 3339 - 3344
反应条件
zirconium tetrachloride in hexane T=20°C; Ring cleavage; alkylation; 0.5 h;
参考文献
Russian Chemical Bulletin, , vol. 48, # 8 p. 1530 - 1532
参考文献
Journal of the American Chemical Society, , vol. 81, p. 6087
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2255;engl.Ausg.S.2156
反应条件
indium trifluoromethanesulfonate
T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
