2,3,4,5,6-五氟溴化苄合成路线 （共 48 条）
反应条件
silver fluoride 1.) diglyme, 3h, 35 deg C, 2.) 35 deg C, 3 d; Yield given. Multistep reaction;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 331 - 347
反应条件
potassium cyanide in ethanol T=75 - 80°C; 0.75 h;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1837 - 1841
反应条件
tetrabutyl-ammonium chloride in tetrahydrofuran; water 0.166667 h;
参考文献
Nakayama, Yasuhide; Inukai, Kazuo; Hayashi, Koichiro; Irie, Masahiro
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1226 - 1230
反应条件
in ethanol; water T=50°C; 5 h;
参考文献
Giese, Michael; Albrecht, Markus; Wiemer, Katharina; Valkonen, Arto; Rissanen, Kari
New Journal of Chemistry, 2012 , vol. 36, # 6 p. 1368 - 1372
反应条件
in ethanol T=75 - 80°C; 0.75 h;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1837 - 1841
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
1.1: 76 percent / potassium phthalimide / dimethylformamide / 130 °C 2.1: hydrazine / ethanol / 2 h / Heating 2.2: 46 percent / aq. HCl / dimethylformamide / 0.5 h / Heating View Scheme
参考文献
Doyon, Jeffrey B.; Jain, Ahamindra
Organic Letters, 1999 , vol. 1, # 2 p. 183 - 185
反应条件
1: (i) NaOEt, EtOH, (ii) /BRN= 647808/, DMF 2: aq. HCl View Scheme
参考文献
Filler,R. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 3 p. 534 - 538
反应条件
1.) via its sodium salt, 2.) hydrolysis; Multistep reaction;
参考文献
Beguin, Claude; Hamman, Sylvain
Organic Magnetic Resonance, 1981 , vol. 16, # 2 p. 129 - 132
反应条件
potassium carbonate in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Sohn, Chang Ho; Chung, Cheol K.; Yin, Sheng; Ramachandran, Prasanna; Loo, Joseph A.; Beauchamp, J. L.
Journal of the American Chemical Society, 2009 , vol. 131, p. 5444 - 5459
