(R)-(-)-2-甲氧基-2-苯乙醇合成路线 (共 46 条)
反应条件
1: DIBAH / diethyl ether / 3 h / -78 °C 2: LiAlH4 / diethyl ether / 1.5 h / Heating View Scheme
参考文献
Australian Journal of Chemistry, , vol. 43, # 12 p. 2045 - 2062
反应条件
cerium(IV) triflate T=80°C; 0.75 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
cerium(IV) triflate T=80°C; 0.75 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
cerium(IV) triflate T=25°C; 1 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
cerium(IV) triflate T=80°C; 1 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
cerium(IV) triflate T=85°C; 4 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
1: 86 percent / pyridine, DMAP / CH2Cl2 / 15 h / Heating 2: 74 percent / toluene / Heating 3: 95 percent / Et3N / CH2Cl2 / Ambient temperature 4: Rh2(OAc)4 / CH2Cl2 / Ambient temperature 5: 65 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 14 p. 4449 - 4460
反应条件
1: 74 percent / toluene / Heating 2: 95 percent / Et3N / CH2Cl2 / Ambient temperature 3: Rh2(OAc)4 / CH2Cl2 / Ambient temperature 4: 65 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 14 p. 4449 - 4460
反应条件
1: Rh2(OAc)4 / CH2Cl2 / Ambient temperature 2: 65 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 14 p. 4449 - 4460
反应条件
1: 95 percent / Et3N / CH2Cl2 / Ambient temperature 2: Rh2(OAc)4 / CH2Cl2 / Ambient temperature 3: 65 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 14 p. 4449 - 4460