3,3-二甲基-2,2-联吡啶合成路线 （共 8 条）
反应条件
1: With magnesium in tetrahydrofuran T=20°C; Grignard Reaction; 0.5 h; Inert atmosphereReflux; 2: With dilithium tetrachlorocuprate(II); oxygen in tetrahydrofuran T=20°C; 2 h;
参考文献
Hua, Si-Kai; Hu, Qiu-Peng; Ren, Jiangmeng; Zeng, Bu-Bing
Synthesis (Germany), 2013 , vol. 45, # 4 art. no. SS-2012-H0751-OP, p. 518 - 526
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
iron(III) chloride T=330°C;
参考文献
Case
Journal of the American Chemical Society, 1946 , vol. 68, p. 2574,2576
反应条件
1: bromine; aqueous sodium nitrite solution; aqueous hydrobromic acid 2: copper / 240 °C View Scheme
参考文献
Case
Journal of the American Chemical Society, 1946 , vol. 68, p. 2574,2576
反应条件
1: phosphorus (III)-bromide / 190 °C 2: copper / 240 °C View Scheme
参考文献
Case
Journal of the American Chemical Society, 1946 , vol. 68, p. 2574,2576
反应条件
in methanol T=20°C; 96 h;
参考文献
Uchida, Yuzuru; Matsumoto, Masami; Kawamura, Haruyasu
Heteroatom Chemistry, 2003 , vol. 14, # 1 p. 72 - 81
参考文献
Case
Journal of the American Chemical Society, 1946 , vol. 68, p. 2574,2576
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; 3 h;
参考文献
Shiina, Isamu
Patent: US2009/62548 A1, 2009 ;
Location in patent: Page/Page column 4 ;
