(4-硝基-苯基)-磷酸二乙酯合成路线 (共 9 条)
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; palladium diacetate; triethylamine in tetrahydrofuran T=68°C; 4 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 18 p. 3207 - 3216
反应条件
N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=70°C; 5 h; in sealed tube;
参考文献
Journal of the American Chemical Society, , vol. 109, # 9 p. 2831 - 2833
反应条件
palladium diacetate; caesium carbonate; potassium iodide in acetonitrile T=20 - 80°C; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 20 p. 4518 - 4520
反应条件
magnesium monoperoxyphthalate hexahydrate in water T=25°C; 24 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 54, # 1/4 p. 221 - 224
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine T=130°C; 20 h; Green chemistry;
参考文献
Journal of Chemical Research, , vol. 37, # 6 p. 359 - 361
反应条件
triethylamine; palladium; triphenylphosphine
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 21, p. 197 - 204
参考文献
Journal of the American Chemical Society, , vol. 77, p. 920
反应条件
phosphorus pentachloride T=110 - 120°C;
参考文献
Sorensen, Morten Dahl; Blaehr, Lars K. A.; Christensen, Mette K.; Hoyer, Thomas; Latini, Scilla; Hjarnaa, Pernille-Julia V.; Bjoerkling, Fredrik
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 24 p. 5461 - 5484
反应条件
stannous chloride in dichloromethane
参考文献
Weigele, Manfred; Sawyer, Tomi K.; Bohacek, Regine; Shakespeare, William C.; Sundaramoorthi, Rajeswari; Wang, Yihan; Dalgarno, David C.; Metcalf III, Chester A.
Patent: US2002/68721 A1, 2002 ;