2,2,4,4,6,6-六甲基-1,2,4,6-氧杂三硅杂环己烷合成路线 (共 6 条)
反应条件
hydrogenchloride in ethanol
参考文献
Gmelin Handbook: Si: MVol.C, 108, page 298 - 303
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Dow Corning Corp.
Patent: DE863943 , 1952 ;
C, 1953 , p. 6179
参考文献
Mironov,V.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1972 , vol. 42, p. 1361 - 1365,1354 - 1357
反应条件
water 1.) 560 deg C, 2.) 10 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gusel'Nikov, L. E.; Volkova, V. V.; Avakyan, V. G.; Volnina, E. A.; Zaikin, V. G.; et al.
Journal of Organometallic Chemistry, 1984 , vol. 271, # 1-3 p. 191 - 206
反应条件
water 1.) 560 deg C, 2.) 10 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gusel'Nikov, L. E.; Volkova, V. V.; Avakyan, V. G.; Volnina, E. A.; Zaikin, V. G.; et al.
Journal of Organometallic Chemistry, 1984 , vol. 271, # 1-3 p. 191 - 206
反应条件
oxygen T=519.9°C; P=0.6 Torr; Ea; Rate constantThermodynamic dataMechanism;
参考文献
Davidson, Iain M. T.; Dean, Christopher E.; Lawrence, F. Timothy
Journal of the Chemical Society, Chemical Communications, 1981 , # 2 p. 52 - 53
反应条件
T=560°C; and their hydrolysates; other substituted cyclosilthianes; reaction in the stream of helium; Product distribution;
参考文献
Gusel'Nikov, L. E.; Volkova, V. V.; Avakyan, V. G.; Volnina, E. A.; Zaikin, V. G.; et al.
Journal of Organometallic Chemistry, 1984 , vol. 271, # 1-3 p. 191 - 206