(1-叔丁基乙烯氧基)三甲基硅烷合成路线 （共 67 条）
反应条件
1: 86 percent / benzene / 4 h / 10 - 15 °C / Irradiation
2: 51 percent / p-toluenesulfonic acid / CCl4; methanol / 24 h / Ambient temperature
3: 90 percent Chromat. / CCl4, diphenylmethane / 1 h / 200 °C
View Scheme
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
(i) PCl5, benzene, (ii) SO2; Multistep reaction;
参考文献
Lazukina,L.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 9 p. 2006 - 2011,1931 - 1935
反应条件
fluorine in chloroform; water; acetonitrile
T=0 - 20°C;
参考文献
Dayan, Sharon; Bareket, Yifat; Rozen, Shlomo
Tetrahedron, 1999 , vol. 55, # 12 p. 3657 - 3664
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride
1.) CH2Cl2, room temperature, 10 h, 2.) THF, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Matano, Yoshihiro; Azuma, Nagao; Suzuki, Hitomi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1739 - 1748
反应条件
bis-(trifluoromethylsulphonyl)amine in acetonitrile
T=20°C;
参考文献
Devineau, Alice; Pousse, Guillaume; Taillier, Catherine; Blanchet, Jerome; Rouden, Jacques; Dalla, Vincent
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2881 - 2886
反应条件
in dichloromethane
168 h; Ambient temperature;
参考文献
Rathore, Rajendra; Kochi, Jay K.
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 627 - 639
参考文献
Anisimova, N. A.; Orlova, N. K.; Shipov, A. G.; Belavin, I. Yu.; Baukov, Yu. I.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 6 p. 1433 - 1434,1278 - 1279
