氯甲酸-2,2,2-三氯乙酯合成路线 （共 61 条）
反应条件
1: 3-amino-5-tert-butyl-2-(p-tolyl)-2H-pyrazole hydrochloride With sodium hydroxide in water; ethyl acetate T=0°C; 1 h; 2: β,β,β-trichloroethoxycarbonylchloride in ethyl acetate T=20°C; 2 h;
参考文献
TORAY INDUSTRIES, INC.
Patent: US2012/184735 A1, 2012 ;
Location in patent: Page/Page column 37 ;
反应条件
sodium hydroxide in water; ethyl acetate
参考文献
Munson, Mark; Mareska, David A.; Kim, Youngboo; Groneberg, Robert D.; Rizzi, James; Rodriguez, Martha; Kim, Ganghyeok; Vigers, Guy; Rao, Chang; Balachari, Devan; Harvey, Darren
Patent: US2004/192653 A1, 2004 ;
US 20040192653 A1
反应条件
hydrazine in chloroform T=0°C; 1 h;
参考文献
Evans, David A.; Johnson, Douglas S.
Organic Letters, 1999 , vol. 1, # 4 p. 595 - 598
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water T=0 - 20°C; Shotten-Baumann reaction;
参考文献
Kaname; Mashige; Yoshifuji
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 5 p. 531 - 536
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3233 - 3236
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3233 - 3236
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3233 - 3236
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3233 - 3236
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3233 - 3236
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
3 h;
参考文献
Chen, Shu-Hui; Huang, Stella; Wei, Jianmei; Farina, Vittorio
Tetrahedron, 1993 , vol. 49, # 14 p. 2805 - 2828
