potassium hydroxide in methanol; diethyl ether byproducts: N2; addn. of MeOH to KOH (65°C), dropwise addn. of diazald in ether, refluxing), addn. of suspn. of HgCl2 in ether (0°C, ice-bath), pptn.; removal of solvent (evapn.), recrystn. (MeOH); elem. anal.;

暂无反应条件数据

in hexadeuterioacetone Kinetics; byproducts: ClSi(OCH2CH2)3N; not isolated, reaction followed by (1)H-NMR spectroscopy;

in dichloromethane room temp., 16 h; standing (28 h), preparative t.l.c.;

in dichloromethane room temp., 3 days; preparative t.l.c.; (1)H-NMR spectroscopy;

iodine