(S)-N-BOC-2-氨基-3-苯丙氰合成路线 （共 13 条）
反应条件
in N,N-dimethyl-formamide T=60°C; 5 h;
参考文献
WO2010/86366 A1, ;
Page/Page column 40 ;
WO 2010/086366 A1
反应条件
in N,N-dimethyl-formamide T=60°C; 3 h; Yield given;
参考文献
Organic Preparations and Procedures International, , vol. 26, # 5 p. 599 - 602
反应条件
in N,N-dimethyl-formamide T=55°C; 22 h;
参考文献
Tetrahedron Letters, , vol. 40, # 13 p. 2629 - 2632
反应条件
1: pyridine / CHCl3 / 22 h 2: 80 percent / dimethylformamide / 22 h / 55 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 13 p. 2629 - 2632
反应条件
in N,N-dimethyl-formamide T=100°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 52, # 51 p. 6968 - 6970
反应条件
1: tetrahydrofuran / Ambient temperature 2: TEA / CH2Cl2 / Ambient temperature 3: dimethylsulfoxide / 45 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 134, # 7 p. 713 - 718
反应条件
in dichloromethane 4 h; Heating;
参考文献
Tetrahedron, , vol. 51, # 45 p. 12337 - 12350
反应条件
1: tetrahydrofuran / Ambient temperature 2: TEA / CH2Cl2 / Ambient temperature 3: dimethylsulfoxide / 45 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 134, # 7 p. 713 - 718
反应条件
1: sodium tetrahydroborate; sulfuric acid / tetrahydrofuran / 18 h / 27 °C 2: thionyl chloride / ethylene glycol dimethyl ether / 4 h / 85 °C 3: sodium hydroxide / tetrahydrofuran / 20 h / 26 °C 4: N,N-dimethyl-formamide / 0.5 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 51 p. 6968 - 6970
反应条件
1: sodium hydroxide / tetrahydrofuran / 20 h / 26 °C 2: N,N-dimethyl-formamide / 0.5 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 51 p. 6968 - 6970
