3-(二甲基氨基)-N,N-二甲基丙酰胺合成路线 (共 10 条)
反应条件
alumina N611N T=150°C; P=2250.23 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
Idemitsu Kosan Co., Ltd.
Patent: EP2426103 A1, 2012 ;
Location in patent: Page/Page column 19; 20 ;
反应条件
2,6-di-tert-butyl-4-methyl-phenol in water T=85°C; 2.5 h;
参考文献
Nicholas, Paul P.
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5266 - 5272
反应条件
in dichloromethane T=0°C; 0.5 h;
参考文献
Hosomi, Akira; Yanagi, Toshiharu; Hojo, Makoto
Tetrahedron Letters, 1991 , vol. 32, # 21 p. 2371 - 2374
参考文献
Erickson
Journal of the American Chemical Society, 1952 , vol. 74, p. 6281
参考文献
Stenlake; Waigh; Dewar; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 3 p. 273 - 276
参考文献
Smirnova,N.V. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, # 8 p. 1756 - 1760,1673 - 1676
参考文献
Stenlake; Waigh; Dewar; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 3 p. 273 - 276
参考文献
Nuzhdin, Kirill B.; Kobzarenko, Aleksei V.; Barabanov, Igor I.; Feldman, Vladimir I.
Mendeleev Communications, 2009 , vol. 19, # 5 p. 268 - 269
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 37, # 8 p. 1756 - 1760,1673 - 1676
反应条件
cupferron; hydroquinone; alumina N611N in water T=250°C; P=2250.23 Torr; 5 h; Product distribution / selectivity;
参考文献
Idemitsu Kosan Co., Ltd.
Patent: EP2426103 A1, 2012 ;
Location in patent: Page/Page column 20-21; 23 ;