(1-苯基-1-丁烯)苯合成路线 （共 59 条）
反应条件
(i) Mg, Et2O, (ii) NH4Cl, H2O; Multistep reaction;
参考文献
Howden,M.E.H. et al.
Journal of the American Chemical Society, 1966 , vol. 88, p. 1732 - 1742
反应条件
water in tetrahydrofuran
1.) -100 deg C, 5 min;
参考文献
Satoh; Takano; Someya; Matsuda
Tetrahedron Letters, 1995 , vol. 36, # 39 p. 7097 - 7100
反应条件
1: 76 percent / NaH / benzene / Ambient temperature
2: 32 percent / solid / 180 - 200 °C / 0.1 Torr
3: benzene / 96 h / Irradiation
View Scheme
参考文献
Koppes, Margareth J. C. M.; Crabbendam, Astrid M.; Cerfontain, Hans
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 11 p. 676 - 683
反应条件
1.1: tetrahydrofuran / 3 h / 60 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / toluene / 2 h / 120 °C / Inert atmosphere
View Scheme
参考文献
He, Zhiheng; Kirchberg, Sylvia; Froehlich, Roland; Studer, Armido
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3699 - 3702
反应条件
in diethyl ether; hexane
6 h; Heating;
参考文献
Chu, Cheng-Ming; Liu, Ju-Tsung; Lin, Wen-Wei; Yao, Ching-Fa
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 1 p. 47 - 52
反应条件
ZnCl2*Et2O
T=-78°C; Rate constant;
参考文献
Mayr, Herbert; Pock, Rudolf
Chemische Berichte, 1986 , vol. 119, # 8 p. 2473 - 2496
反应条件
potassium tert-butylate; magnesium
Yield given. Multistep reaction;
参考文献
Hernandez, David; Larson, Gerald L.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4285 - 4287
反应条件
water; ethyl magnesium chloride
1.) THF, 0 deg C, 30 min.; Yield given. Multistep reaction;
参考文献
Satoh, Tsuyoshi; Takano, Koji; Hiroyuki, Ota; Someya, Hideaki; Matsuda, Kenji; Koyama, Mai
Tetrahedron, 1998 , vol. 54, # 21 p. 5557 - 5574
反应条件
lithium
1.) Et2O, -20 deg C, 5 h, 2.) Et2O, room temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Maercker, Adalbert; Daub, Volker E. E.
Tetrahedron, 1994 , vol. 50, # 8 p. 2439 - 2458
反应条件
(i), (ii) aq. H2SO4; Multistep reaction;
参考文献
Boyce,R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1292 - 1295
