P-[(4-溴苯基)甲基]-膦酸二甲酯合成路线 （共 7 条）
参考文献
Lei, Yao; Wrobleski, Aaron D.; Golden, Jennifer E.; Powell, Douglas R.; Aube, Jeffrey
Journal of the American Chemical Society, 2005 , vol. 127, # 13 p. 4552 - 4553
反应条件
sodium hydride in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Witt, Dariusz; Rachon, Janusz
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 108, # 1-4 p. 169 - 187
反应条件
RefluxInert atmosphere;
参考文献
Lefebvre, Quentin; Jentsch, Marc; Rueping, Magnus
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1883 - 1890
反应条件
1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / |Inert atmosphere 2: iodine / tetrahydrofuran; toluene / |Inert atmosphere; |Flow reactor; |Irradiation View Scheme
参考文献
Lefebvre, Quentin; Jentsch, Marc; Rueping, Magnus
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1883 - 1890
反应条件
1: sodium hydride 2: n-butyllithium / tetrahydrofuran / -78 - 20 °C / Inert atmosphere View Scheme
参考文献
Liang, Zuo-Qin; Li, Ye-Xin; Yang, Jia-Xiang; Ren, Yan; Tao, Xu-Tang
Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1329 - 1333
参考文献
Liang, Zuo-Qin; Li, Ye-Xin; Yang, Jia-Xiang; Ren, Yan; Tao, Xu-Tang
Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1329 - 1333
反应条件
potassium tert-butylate in tetrahydrofuran
T=0 - 20°C; Horner-Wadsworth-Emmons Olefination; Inert atmosphere;
参考文献
Lefebvre, Quentin; Jentsch, Marc; Rueping, Magnus
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1883 - 1890
