(二甲基苯基甲硅烷基)乙酰亚基合成路线 （共 7 条）
反应条件
in tetrahydrofuran T=0 - 20°C;
参考文献
Hasegawa, Munehiro; Murakami, Masahiro
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3764 - 3769
反应条件
ethylmagnesium bromide in tetrahydrofuran 36 h; Heating;
参考文献
Denmark, Scott E.; Habermas, Karl L.; Hite, Gary A.; Jones, Todd K.
Tetrahedron, 1986 , vol. 42, # 11 p. 2821 - 2829
参考文献
Tetrahedron, , vol. 63, # 1 p. 224 - 231
反应条件
1: [dimethyl(phenyl)silyl]acetylene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; 2: N,O-dimethylacetohydroxamic acid in tetrahydrofuran; hexane T=-78 - 20°C; 2.5 h; Further stages.;
参考文献
Schubert, Thomas; Hummel, Werner; Kula, Maria-Regina; Mueller, Michael
European Journal of Organic Chemistry, 2001 , # 22 p. 4181 - 4187
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene); water in benzene-d6 T=40°C; Inert atmosphere;
参考文献
Powala, Beata; Fischer, Helmut; Pietraszuk, Cezary
Dalton Transactions, 2010 , vol. 39, # 8 p. 1923 - 1925
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.33 h / -78 °C 1.2: 87 percent / tetrahydrofuran / 1.5 h / -78 °C 2.1: 93 percent / Red-Al / diethyl ether; toluene / 4 h / 20 °C 3.1: 51 percent / TFAA; Et3N / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Jung, Michael E.; Piizzi, Grazia
Journal of Organic Chemistry, 2002 , vol. 67, # 11 p. 3911 - 3914
反应条件
Wilkinson's catalyst in toluene 60 h; Ambient temperature;
参考文献
Ohshita, Joji; Furumori, Kenji; Matsuguchi, Akira; Ishikawa, Mitsuo
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3277 - 3280
