三丁基(4-氯苯基)锡烷合成路线 （共 30 条）
反应条件
n-butyllithium in tetrahydrofuran
参考文献
Rutgers, The State University of New Jersey
Patent: US5770617 A1, 1998 ;
反应条件
niobium bromide in N,N,N',N',N'',N''-hexamethylphosphoric triamide 17 h, 10 mole-percent NiBr2 as catalyst;
参考文献
Bumagin, N. A.; Gulevich, Yu. V.; Artamkina, G. A.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1098
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1195
反应条件
magnesium in diethyl ether refluxing, 8h;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.5.6, page 318 - 322
反应条件
[PdBr2(PPh3)2] in toluene byproducts: (p-ClC6H4)2, Bu3SnBr; at 115°C for 15 h in sealed thick wall Pyrex glass ampoules;
参考文献
Azizian, Hormoz; Eaborn, Colin; Pidcock, Alan
Journal of Organometallic Chemistry, 1981 , vol. 215, # 1 p. 49 - 58
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene byproducts: Bu3SnBr, Me3SiBr; at 115°C for 15 h in sealed thick wall Pyrex glass ampoules;
参考文献
Azizian, Hormoz; Eaborn, Colin; Pidcock, Alan
Journal of Organometallic Chemistry, 1981 , vol. 215, # 1 p. 49 - 58
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 2.33333 h; Product distribution;
参考文献
Bumagin, N. A.; Gulevich, Yu. V.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1044 - 1049
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1137 - 1142
反应条件
in tetrahydrofuran Bu3SnCl and Grignard reagent in THF; distn. under reduced pressure;
参考文献
Uemura; Ohe; Motofusa
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 7 p. 1343 - 1348
反应条件
Yield given. Multistep reaction;
参考文献
Owton; Brunavs
Synthetic Communications, 1991 , vol. 21, # 8-9 p. 981 - 987
反应条件
(tBuCN)2CuOTf; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate in ethyl acetate T=25°C; 12 h; Inert atmosphereGlovebox;
参考文献
Ye, Yingda; Sanford, Melanie S.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4648 - 4651
反应条件
copper dichloride; palladium dichloride in acetic acid T=25°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 7 p. 1343 - 1348
