1-甲基-1,2-环氧环己烷合成路线 (共 60 条)
反应条件
sodium tetrahydridoaluminate in tetrahydrofuran T=0°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Cha, Jin Soon; Brown, Herbert C.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4727 - 4731
反应条件
zinc(II) iodide in dichloromethane 48 h; Heating;
参考文献
Gassman, Paul G.; Haberman, Leonard M.
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 5010 - 5013
反应条件
trifluoroacetic acid; phenylselenocarboxamide in dichloromethane T=0°C; 0.0833333 h; With other reagents are dicussed.; Mechanism;
参考文献
Ogawa, Akiya; Miyake, Jun-ichi; Murai, Shinji; Sonoda, Noboru
Tetrahedron Letters, 1985 , vol. 26, # 5 p. 669 - 672
反应条件
hydrogen; palladium on activated charcoal in isopropyl alcohol T=20°C; P=760 Torr; 4 h; various solvents; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 21 p. 4139 - 4143
反应条件
1: BF3*OEt2 / diethyl ether / 2 h / Ambient temperature 2: 83 percent / Borane / tetrahydrofuran / 2 h / other cond.: ether, Morpholine-borane or Morpholine-borane, BF3 View Scheme
参考文献
Smith, William B.
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3219 - 3220
反应条件
zinc(II) tetrahydroborate; silica gel in tetrahydrofuran 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1334 - 1335
参考文献
Koetz; Hoffmann
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 110, p. 115
反应条件
hydrogen; palladium on activated charcoal in isopropyl alcohol T=20°C; P=760 Torr; 4 h; various solvents; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 21 p. 4139 - 4143
反应条件
morpholine-borane; boron trifluoride diethyl etherate in diethyl ether 2 h; Ambient temperature; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 17 p. 3219 - 3220
反应条件
zinc(II) tetrahydroborate; silica gel in tetrahydrofuran 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1334 - 1335